MS Report from Instrument: LCMS-02 File ..0711 2017-07-11 08-08-28\\BIA2017-711-WYQ2.D Tgt Mass (CHM): Injection Date : 11 Jul 17 4:06 pm +0800 Seq. Line : 101 Sample Name : BIZ2017-711-WYQ2 Location : P2-A-02 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20170711\\20170711 2017-07-11 08-08-28\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170711\\20170711 2017-07-11 08-08-28\\1-POS-3MIN.M Catalog No : HY-102014 Batch#25327 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off 75050025000.5 DAD1 C, Sig=2,4 Ref=off mAU30020010000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701500001000005000000.51 Ion 381, MSD1 381,Target Mass 380 +H Positive, EIC=380.7:381.7 8000060000400002.1372.1912.2152.2482.2882.6032.6692.3650.6931.72.5082000002.8502..99531222.984min1.522.0552.5min1.51.6111.8012.1002.16811.4581.8012.1682.028mAU1.522.0282.5min22.0552.5min0.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5 RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.46 0.03 3.27 1.75 0.20 117 1.80 0.03 3.94 2.27 0.24 117 2.03 0.03 1657.12 1040.83 99.01 381 2.17 0.02 9.29 7.53 0.55 117 Integration Results for DAD1 C, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.61 0.02 0.24 0.26 0.04 117 1.80 0.03 1.51 0.85 0.22 117 2.03 0.03 673.79 422.38 99.08 381 2.10 0.02 1.57 1.74 0.23 117 2.17 0.02 2.93 2.36 0.43 117 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|LCMS-02 7/12/2017 9:02:18 ZLJ_587Page 1 of 3
MS Report from Instrument: LCMS-02 2.05 0.04 404472.47 155513.00 100.00 381LCMS-02 7/12/2017 9:02:18 ZLJ_587Page 2 of 3
MS Report from Instrument: LCMS-02Ret. Time: 2.05 <<<< POSITIVE SPECTRA >>>> ES-API Positive 381.1 404.0 403.0 117.2 383.0300002500020000150001000050000200300400500600700800900m/zLCMS-02 7/12/2017 9:02:18 ZLJ_587Page 3 of 3
